Search results for "Structural analysi"
showing 10 items of 38 documents
I Telamoni del Tempio di Zeus ad Agrigento: rilievi, disegni e ricostruzioni
2013
Oggetto dello studio qui presentato è la ricostruzione di un intercolumnio del fronte esterno del Tempio di Zeus ad Agrigento, basata sul rilievo del Telamone oggi custodito presso il Museo Archeologico, sugli studi e i numerosi saggi di ricostruzione proposti dagli studiosi dal XVIII secolo fino alla metà dello scorso secolo e sulla analisi strutturale del Telamone ricostruito nel Museo. The drawings of the telamones, the giant statues placed the front of the Temple of Zeus in the archaeological area of Agrigento, have fascinated some of the most famous neoclassical architects in Europe. The virtual reconstruction of one intercolumnial of the Temple, based both on the range-based survey of…
Biosilicification of loricate choanoflagellate: organic composition of the nanotubular siliceous costal strips of Stephanoeca diplocostata.
2010
SUMMARY Loricate choanoflagellates (unicellular, eukaryotic flagellates; phylum Choanozoa) synthesize a basket-like siliceous lorica reinforced by costal strips (diameter of approximately 100 nm and length of 3 μm). In the present study, the composition of these siliceous costal strips is described, using Stephanoeca diplocostata as a model. Analyses by energy-dispersive X-ray spectroscopy (EDX), coupled with transmission electron microscopy (TEM), indicate that the costal strips comprise inorganic and organic components. The organic, proteinaceous scaffold contained one major polypeptide of mass 14 kDa that reacted with wheat germ agglutinin. Polyclonal antibodies were raised that allowed …
Multiscale microstructural characterization of particulate-reinforced composite with non-destructive X-ray micro- and nanotomography
2018
Abstract Methods based on X-ray tomography are developed to study the relevant statistical quantities describing the microstructural inhomogeneity of particulate reinforced composites. The developed methods are applied in estimating microstructural inhomogeneity parameters of composites containing metallic glass particles in metal matrix, extruded in varying pressure loads. This study indicates that the critical characteristics with regard to the effect of particle clustering are cluster size and shape, local volume fraction of particles in the cluster and the distance between clusters. The results demonstrate that the spatial distribution of reinforcement is very uneven and the amount of p…
Analysis of non-uniform torsion in curved incrementally launched bridges
2014
Abstract Incremental launching is a common and convenient methodology to build continuous girder bridges on several piers. Although it has mainly been applied to straight bridges with box sections, today it is also used for construction of horizontally curved bridges with concrete and composite steel–concrete closed or open sections like I-girders. In these cases the contribution of torsion to the stress state becomes of primary importance when the construction stages of these bridges are analysed. Moreover, the presence of thin-walled cross-sections, makes the analysis of non-uniform torsion fundamental when the angle of twist per unit length is not constant or warping is prevented in thos…
A structural comparison of halloysite nanotubes of different origin by Small-Angle Neutron Scattering (SANS) and Electric Birefringence
2018
The structure of halloysite nanotubes (Hal) from different mines was investigated by Small-Angle Neutron Scattering (SANS) and Electric Birefringence (EBR) experiments. The analysis of the SANS curves allowed us to correlate the sizes and polydispersity and the specific surfaces (obtained by a Porod analysis of the SANS data) of the nanotubes with their specific geological setting. Contrast matching measurements were performed on patch Hal (from Western Australia) in order to determine their experimental scattering length density for a more precise analysis. Further characterization of the mesoscopic structure of Hal was carried out by Electric Birefringence (EBR), which allowed to study th…
Problemas multiplicativos relacionados con la división de fracciones : un estudio sobre su enseñanza y aprendizaje
2013
Los estudiantes tienen dificultades para asociar el enunciado de un problema multiplicativo con la operación que permite resolverlo; esta investigación identifica los tipos de problemas multiplicativos que los estudiantes reconocen como de división de fracciones. Mediante el análisis histórico-epistemológico de textos de enseñanza sobre tres épocas históricas y ocho períodos diferentes, se obtiene un listado de variables de enseñanza (algoritmos, sentidos de uso de fracción y de división de fracciones, representaciones, problemas), así como los valores de dichas variables. Se localizan en los textos consultados algunas reglas particulares y seis algoritmos generales, cuyo predominio ha vari…
Synthesis and structural studies on Ni(II) dithiocarbamates : Exploring intramolecular Ni···H-C interactions
2017
Five new Ni(II) dithiocarbamates with NiS4, NiS2PN and NiS2PCl coordination spheres, viz. [Ni(bupmbzdtc)2] (1), [Ni(bupmbzdtc)(PPh3)(NCS)] (2), [Ni(bupmbzdtc)(PPh3)Cl] (3), [Ni(4-dpmpzdtc)(PPh3)Cl] (4) and [Ni(pbbzbudtc)(PPh3)(NCS)] (5), where bupmbzdtc = N-butyl(p-methylbenzyl)dithiocarbamato anion, 4-dpmpzdtc = 4-(diphenylmethyl)piperazinecarbodithioato anion, pbbzbudtc = N-(p-bromobenzyl)butyl-dithiocarbamato anion and PPh3 = triphenylphosphine, were synthesized and characterized by UV, IR, NMR and single crystal X-ray diffraction methods. Spectral results suggest a square planar geometry around the Ni(II) metal center for all the synthesized complexes. Single crystal X-ray structural an…
Further improvements in the structural analysis of DEMO Divertor Cassette body and design assessment according to RCC-MRx
2019
Abstract This paper presents the enhancements related to the structural analyses of DEMO Divertor in the framework of the EUROfusion Power Plant Physics & Technology (PPPT) program. This activity started two years ago and its preliminary results were published in previous papers. It has been divided in some areas defined by the similarity of the matters they contain: the structural analysis, of utmost importance, has been preceded by a preliminary phase, like the geometry definition or the thermal and the electric-magnetic analysis for loads evaluation; then the structural analysis has been finally confirmed with further evaluations related to excessive deformation or plastic instability. T…
A perturbation approach for the response of dynamically modified structural systems
1998
The problem of the structural analysis under changes of dynamical parameters is of particular interest. This is due to the fact that often the real structures are different from the predicted ones. In this paper, an unconditionally stable step-by-step procedure, able to evaluate the deterministic response of linear structures with modifications, is presented. The proposed procedure requires the evaluation of the transition matrix, which is the fundamental operator of the step-by-step solution, by means of a perturbation approach. This technique overcomes the difficulties connected with the evaluation of the eigenproperties of the modified structures usually required to obtain the transition…
Activation of the Cyano Group at Imidazole via Copper Stimulated Alcoholysis
2019
Reactions of 4,5-dicyano-1-methylimidazole with CuX2 (X = Cl, Br) in alcohol solvents (ethanol and methanol) resulted in the formation of Cu(II) carboximidate complexes [CuCl2(5- cyano-4-C(OEt)N-1-methylimidazole)(EtOH)] (1), [Cu2(µ